凈化濕法磷酸制備六偏磷酸鈉過程-河南東福環?？萍加邢薰?/title> <meta name="keywords" content="凈化濕法磷酸制備六偏磷酸鈉過程"> <meta name="description" content="在磷酸制備的兩條傳統路線中,熱法路線制備的磷酸純度高,多用于精細磷酸鹽產品的制備,但能耗和成本高限制了其發展潛力。濕法磷酸生產成本低,但由于其雜質含量高,難以直接用作工業磷酸或食品磷酸,必須經過凈化處理。經過溶劑萃取等凈化手段處理過的濕法磷酸,純度達到或接近熱法磷酸,且凈化后的成本仍然較低,近年來越來越多地取代熱法磷酸..."> <link rel="stylesheet" href="/template/default/index/css/animate.min.css"> <link rel="stylesheet" href="/template/default/index/css/swiper.min.css"> <link rel="stylesheet" href="/template/default/index/css/yunu.css"> <script src="/template/default/index/js/jquery.min.js"></script> <script src="/template/default/index/js/wow.min.js"></script> <script src="/template/default/index/js/swiper.min.js"></script> <script src="/template/default/index/js/yunu.js"></script> <meta http-equiv="Cache-Control" content="no-transform" /> <meta http-equiv="Cache-Control" content="no-siteapp" /> </head> <body> <div style="position:fixed;left:-9000px;top:-9000px;"><menu id="b35jz"><li id="b35jz"><td 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<span>您的位置：</span> <a href="http://www.quickcapitallending.com/">首頁</a>>><a href="http://www.quickcapitallending.com/news/">新聞中心</a>>><a href="http://www.quickcapitallending.com/news/hydt/">行業動態</a> </div> 行業動態 </div> <div class="content-title"> <h1>凈化濕法磷酸制備六偏磷酸鈉過程</h1> <p> <span>時間：2021-02-09 15:21:38</span> <span>來源：http://www.quickcapitallending.com</span> <span>點擊：150575次</span> </p> </div> <div class="content-body"> <p>在磷酸制備的兩條傳統路線中,熱法路線制備的磷酸純度高,多用于精細磷酸鹽產品的制備,但能耗和成本高限制了其發展潛力。濕法磷酸生產成本低,但由于其雜質含量高,難以直接用作工業磷酸或食品磷酸,必須經過凈化處理。經過溶劑萃取等凈化手段處理過的濕法磷酸,純度達到或接近熱法磷酸,且凈化后的成本仍然較低,近年來越來越多地取代熱法磷酸成為制備精細磷酸鹽產品的原料。本文以<a href='http://www.quickcapitallending.com' target='_blank' title='六偏磷酸鈉' ><strong>六偏磷酸鈉</strong></a>作為目標產物,研究了以凈化濕法磷酸制備磷酸鹽的工藝過程。即從負載磷酸的溶劑相直接中和制備磷酸鹽,其步驟包括溶劑萃取凈化工藝、凈化濕法磷酸反萃、<a href='http://www.quickcapitallending.com' target='_blank' title='磷酸二氫鈉' ><strong>磷酸二氫鈉</strong></a>的結晶、<a href='http://www.quickcapitallending.com' target='_blank' title='六偏磷酸鈉' ><strong>六偏磷酸鈉</strong></a>聚合制備。</p><p>主要研究了適用的萃取體系,原料磷酸濃度、溫度、時間等對萃取的影響；考察了反萃過程中的反萃時間、溫度等適當的操作條件,分析和考察了結晶過程中攪拌速率,降溫速率等工藝條件以及來自磷酸中各陰、陽離子對<a href='http://www.quickcapitallending.com' target='_blank' title='磷酸二氫鈉' ><strong>磷酸二氫鈉</strong></a>結晶介穩區的影響,并對SO42-,F-,Fe3+,Al3+,Mg2+等雜質離子含量與<a href='http://www.quickcapitallending.com' target='_blank' title='磷酸二氫鈉' ><strong>磷酸二氫鈉</strong></a>結晶介穩區寬度之間關系進行了擬合；最后實驗研究了<a href='http://www.quickcapitallending.com' target='_blank' title='磷酸二氫鈉' ><strong>磷酸二氫鈉</strong></a>聚合制備<a href='http://www.quickcapitallending.com' target='_blank' title='六偏磷酸鈉' ><strong>六偏磷酸鈉</strong></a>反應的熔融時間和溫度與聚合產物分子量之間的關系。通過實驗,本文采用TBP+煤油為萃取劑,在50℃下萃??；萃取液在25℃下以1mol/L的NaOH等化學當量反萃；反萃后分離萃取劑,將所得負載磷酸二氫鈉溶液濃縮后在單位體積能耗0.1w/L的攪拌條件下以0.2℃/min的降溫速率降溫結晶,制得磷酸二氫鈉晶體在高溫下熔融聚合,得到<a href='http://www.quickcapitallending.com' target='_blank' title='六偏磷酸鈉' ><strong>六偏磷酸鈉</strong></a>產品。 </p><p>在優化的萃取、反萃、結晶、聚合條件下,可制得分子量范圍6000—7000的六偏磷酸鈉聚合產物,其中Fe.As.Pb.F等雜質的含量達到國家食品級要求。與熱法酸工藝相比,此工藝路線可以在保證產品質量的前提下降低原料成本。具有顯著的經濟和社會效益。</p> </div> <ul class="content-exp"> <li><span>上一篇：</span><a href="http://www.quickcapitallending.com/news/hydt/300.html">處理垃圾填埋場滲濾液的膜的污染控制與清洗研究</a></li> <li><span>下一篇：</span><a href="http://www.quickcapitallending.com/news/hydt/302.html">選礦行業油田行業六偏磷酸鈉抑制劑價格</a></li> </ul> </div> </div> </div> </div> <div class="footer"> <div class="container clearfix"> <div class="footer-nav"> <a href="http://www.quickcapitallending.com/">網站首頁</a> <a href="http://www.quickcapitallending.com/pro/1/1/">六偏磷酸鈉</a> <a href="http://www.quickcapitallending.com/pro/1/5/237.html">磷酸二氫鋁</a> <a href="http://www.quickcapitallending.com/pro/1/5/285.html">液體磷酸二氫鋁</a> <a href="http://www.quickcapitallending.com/pro/">產品中心</a> <a href="http://www.quickcapitallending.com/news/">新聞中心</a> <a href="http://www.quickcapitallending.com/case/">客戶案例</a> <a 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